复合材料科学与工程 ›› 2023, Vol. 0 ›› Issue (6): 30-36.DOI: 10.19936/j.cnki.2096-8000.20230628.005

• 基础研究 • 上一篇    下一篇

高温预损伤对碳纤维复合材料冲击后压缩剩余强度影响规律研究

曹雨函1, 郭姝含1, 欧阳俊杰2, 孔繁淇1, 王付胜1*   

  1. 1.中国民航大学 中欧航空工程师学院,天津 300300;
    2.中国商飞上海飞机设计研究院,上海 201210
  • 收稿日期:2022-05-11 出版日期:2023-06-28 发布日期:2023-08-22
  • 通讯作者: 王付胜(1987—),男,实验师,硕士研究生,主要从事复合材料失效分析方面的研究,fswang@cauc.edu.cn。
  • 作者简介:曹雨函(1999—),女,硕士研究生,主要从事复合材料失效分析方面的研究。
  • 基金资助:
    大学生创新创业训练计划项目(202010059030)

Research of the influence of high temperature pre-damage on the residual strength after impact of carbon fiber composites

CAO Yuhan1, GUO Shuhan1, OUYANG Junjie2, KONG Fanqi1, WANG Fusheng1*   

  1. 1. Sino-European Institute of Aviation Engineering, Civil Aviation University of China, Tianjin 300300, China;
    2. COMAC Shanghai Aircraft Design and Research Institute, Shanghai 201210, China
  • Received:2022-05-11 Online:2023-06-28 Published:2023-08-22

摘要: 对9A12环氧树脂基T700级碳纤维复合材料(CFRP)层合板在不同预损伤温度(180 ℃、210 ℃、240 ℃)和损伤时间(24 h、72 h、120 h、168 h)下进行低速冲击和冲击后压缩试验(CAI),结合数字图像技术(DIC)和微观形貌研究高温预损伤下CFRP层合板失重量与剩余强度随损伤温度和时间的变化规律。结果表明:CFRP层合板不同温度下相对失重量和冲击后压缩强度下降率均先快后慢,最后趋于稳定。180 ℃预损伤后相对失重量和剩余强度随损伤时间变化较小,损伤120 h后趋于稳定。温度升至210 ℃与240 ℃,损伤初期层合板剩余强度迅速下降,40 h后剩余强度分别降低20.4%和25.1%,较180 ℃下损伤120 h后剩余强度更低。分析结果,建立CFRP层合板高温预损伤导致的失重量与冲击后压缩剩余强度线性关系模型。利用DIC技术记录CFRP层合板在压缩方向上的应变演化规律,并得到应变云图。观察微观形貌发现高温损伤使树脂对纤维的包裹性下降,层间出现散布的树脂颗粒,且在240 ℃时材料的损伤形式由结构性断裂变为环氧树脂氧化分解导致的损伤。

关键词: 碳纤维复合材料, 高温预损伤, CAI剩余强度, 数字图像相关技术

Abstract: Low-speed impact and post-impact compression test (CAI) were performed on 9A12 epoxy resin based T700 composite (CFRP) laminates at different pre-damage temperatures (180 ℃, 210 ℃, 240 ℃) and damage times (24 h, 72 h, 120 h, 168 h). Digital image technology (DIC) and micro-morphology were used to study the variation of weight loss and residual strength of CFRP laminates with damage temperature and damage time due to high temperature pre-damage. The results show that the relative weight loss rate and the decrease rate of compressive strength after impact of CFRP laminates at different temperatures are firstly fast and gradually slow, and finally tend to be stable. The relative weight loss and residual strength after pre-damage at 180 ℃ changed little with the damage time, and tended to be stable after 120 h of damage. When the temperature rises to 210 ℃ and 240 ℃, the residual strength of the laminate decreases rapidly at the initial stage of damage. After 40 h, the residual strength decreases by 20.4% and 25.1%, respectively, which is lower than that after 120 h of damage at 180 ℃. Based on the analysis of results, a linear relationship model of the weight loss caused by high temperature pre-damage of CFRP laminates and the residual strength after impact is established. The strain evolution law of the CFRP laminate in the compression direction was recorded by DIC technology, and the strain cloud map was obtained. Observing the microstructure, it was found that the high temperature damage reduced the encapsulation of the resin to the fiber, and scattered resin particles appeared between the layers. At 240 ℃, the damage form of the material changed from structural fracture to damage caused by oxidative decomposition of epoxy resin.

Key words: carbon fiber composites, high temperature pre-damage, CAI residual strength, digital image correlation technology

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