玻璃钢/复合材料 ›› 2018, Vol. 0 ›› Issue (9): 23-29.

• 基础研究 • 上一篇    下一篇

厚截面复合材料固化温度不均匀性对力学性能的影响

刘桂铭1, 湛利华1,2*, 陈效平1, 常腾飞2   

  1. 1.中南大学机电工程学院,长沙410083;
    2.中南大学轻合金研究院,长沙410083
  • 收稿日期:2018-01-12 出版日期:2018-09-28 发布日期:2018-09-28
  • 通讯作者: 湛利华(1976-),女,博士,教授,主要从事先进材料制备技术与装备方面的研究,yjs-cast@csu.edu.cn。
  • 作者简介:刘桂铭(1993-),男,硕士,主要从事碳纤维增强热固性树脂复合材料方面的研究。
  • 基金资助:
    国家重点基础研究发展计划(973计划)项目(2014CB046502);中南大学中央高校基本科研业务费专项资金(2018zzts473)

EFFECTS OF THICK COMPOSITE CURING TEMPERATURENON-UNIFORMITY ON MECHANICAL PROPERTIES

LIU Gui-ming1, ZHAN Li-hua1,2*, CHEN Xiao-ping1, CHANG Teng-fei2   

  1. 1.School of Mechanical and Electrical Engineering, Central South University, Changsha 410083, China;
    2.Institute of Light Alloy, Central South University, Changsha 410083, China
  • Received:2018-01-12 Online:2018-09-28 Published:2018-09-28

摘要: 通过对厚截面复合材料层合板不同部位设置隔离膜与热电偶的方法来测试厚截面复合材料在固化过程中沿厚度方向的温度分布。采用横向拉伸和短梁剪切测试手段,研究了厚截面复合材料制件固化过程中沿厚度方向的温度不均匀性对力学性能的影响规律,并通过扫描电子显微镜(SEM)分析了层合板力学性能测试后的断面微观形貌。结果表明,厚截面复合材料固化过程中沿厚度方向存在明显的温度梯度,随着温差的增加,拉伸强度、层间剪切强度力学性能呈下降趋势。以上层合板为参考对象,当层合板沿厚度方向温差为20.6 ℃时,其横向拉伸强度相差7.4%,层间剪切强度相差6.8%;当层合板沿厚度方向温差为10.2 ℃时,其横向拉伸强度相差3.8%,层间剪切强度相差3.4%。这是由于固化温度过高,树脂与碳纤维界面的结合强度降低。该研究为厚截面复合材料制件热压罐成型过程中温度场均匀调控的必要性提供了重要的实验依据及理论参考。

关键词: 厚截面复合材料, 层合板, 温度梯度, 力学性能

Abstract: Temperature gradient distribution of thick composite along the thickness direction in curing process was measured using a method of setting Teflon film and thermocouple monitor in different position. The relationship between temperature non-uniformity and mechanical performance was studied by means of tensile test and shear test. And, laminate micro-structural fracture surface was analyzed by SEM. The results show that there are obvious temperature gradient along the thickness direction in the curing process of thick composite, and the mechanical properties of tensile strength and inter-layer shear strength show a downward trend with the increase of temperature difference. Employing the top laminate as reference, when there is 20.6 degree inner temperature difference in composite laminate tensile, the strength difference is 7.4%, and the shear strength difference is 6.8%. Likewise, when there is 10.2 degree inner temperature difference, the tensile strength difference is 3.8%, and the shear strength difference is 3.4%. This is due to the high curing temperature, and inter-facial strength between resin and carbon fiber reduces. This study provides significant experimental evidence and theoretical reference for the necessity of controlling the composite temperature distribution uniformty for the thick section parts of the composite materials during the autoclave curing.

Key words: thick composite, laminate, temperature gradient, mechanical properties

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